We seek a highly motivated postdoctoral researcher with a strong background in electrocatalysis to join the Center for Nanoscale Materials (CNM) at Argonne National Laboratory. The successful candidate will lead efforts in materials synthesis, in situ/operando characterization, and catalytic performance evaluation. This role offers a unique opportunity to leverage CNM’s advanced characterization capabilities, contribute to high-impact publications, and collaborate with scientists across CNM, Argonne, and external partners. Key Responsibilities Design, synthesize, and rigorously evaluate well-defined electrocatalyst materials Plan and execute in situ/operando studies using advanced techniques such as X-ray Absorption Spectroscopy (XAS), X-ray Photoelectron Spectroscopy (XPS), Raman spectroscopy, Differential Electrochemical Mass Spectroscopy (DEMS), and complementary methods Perform electrochemical testing and benchmarking; analyze and interpret complex datasets to elucidate catalytic mechanisms and structure–property relationships Document results and lead the preparation of high-impact publications; present findings at internal meetings and external conferences Collaborate within a multidisciplinary environment that includes experimentalists, modelers, and data scientists Position Requirements Recent or soon-to-be-completed PhD (within the last 0-5 years) in field of Materials Science, Chemical Engineering, Chemistry, or a related field Demonstrated expertise in electrocatalysis, including catalyst synthesis, electrochemical characterization, and mechanistic analysis Hands-on experience with in situ/operando spectroscopy and/or advanced characterization (e.g., XAS, XPS, Raman, DEMS) Proficiency in data analysis; familiarity with modeling or data science tools is a plus Excellent written and oral communication skills and the ability to work effectively in a collaborative, multidisciplinary team Ability to model Argonne’s core values of impact, safety, respect, integrity, and teamwork Application Materials Curriculum vitae (CV) Cover letter describing research experience and fit for the role Contact information for three references Job Family Postdoctoral Job Profile Postdoctoral Appointee Worker Type Long-Term (Fixed Term) Time Type Full time The expected hiring range for this position is $70,758.00-$117,925.00. Please note that the pay range information is a general guideline only. The pay offered to a selected candidate will be determined based on factors such as, but not limited to, the scope and responsibilities of the position, the qualifications of the selected candidate, business considerations, internal equity, and external market pay for comparable jobs. Additionally, comprehensive benefits are part of the total rewards package. Click here to view Argonne employee benefits! As an equal employment opportunity employer, and in accordance with our core values of impact, safety, respect, integrity and teamwork, Argonne National Laboratory is committed to a safe and welcoming workplace that fosters collaborative scientific discovery and innovation. Argonne encourages everyone to apply for employment. Argonne is committed to nondiscrimination and considers all qualified applicants for employment without regard to any characteristic protected by law. Argonne employees, and certain guest researchers and contractors, are subject to particular restrictions related to participation in Foreign Government Sponsored or Affiliated Activities, as defined and detailed in United States Department of Energy Order 486.1A. You will be asked to disclose any such participation in the application phase for review by Argonne's Legal Department. All Argonne offers of employment are contingent upon a background check that includes an assessment of criminal conviction history conducted on an individualized and case-by-case basis. Please be advised that Argonne positions require upon hire (or may require in the future) for the individual be to obtain a government access authorization that involves additional background check requirements. Failure to obtain or maintain such government access authorization could result in the withdrawal of a job offer or future termination of employment. Interested in translating science into innovation? Build your career at Argonne. At Argonne, we view the world from a different perspective. Our scientists and engineers conduct world-class research in clean energy, the environment, technology, national security and more. We’re finding creative ways to prepare the world for a better future. To learn more about Argonne's benefits programs, amenities, and other employee programs, visit our main Careers site. To learn more about the exciting science going on at Argonne, visit our Science and Technology page. To request a reasonable accommodation or for other application support, contact us anytime at careers@anl.gov or 630-252-2336.